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The concept and materials used in the plastic microchannel technique (PMT) have been reviewed. The microchannels made of more than two layers of plastic films or membranes have a high degree of efficiency and selectivity in separating and purifying organic compounds and/or inorganic ions. The performance of PMT is mainly governed by factors such as the designed configuration, the design of plastic films/membranes, and the structure of channels. The concept and materials used in the preparation of microchannels, the chemical and mechanical strength, and the performance of microchannels have been reviewed in this paper. With the development of microfluidics and micro-materials, the potential of the PMT has broadened. In the past ten years, much work has been done to seek new applications for PMT. Several new applications have been developed as a result, including a method for detecting mercury, an electrochemical method for glucose, a method for quantitative detection of heavy metals, and a method for bio-sensing. PMT is a versatile method that will continue to evolve as researchers try to find new ways to use it.Room temperature preparation of aryl-α-carbamate-Pd/PdOx catalyst for Suzuki-Miyaura cross coupling.
A new room temperature procedure for the synthesis of an aryl-α-carbamate-Pd/PdOx catalyst has been developed. The use of a simple room temperature procedure to prepare aryl-α-carbamate-Pd/PdOx catalysts is reported here for the first time. The catalyst is prepared by reacting a solution of aryl-α-carbamates and PdCl2(PPh3)2 in N,N-dimethylformamide (DMF), and then the palladation of the aryl-α-carbamate occurs under microwave irradiation. The resulting catalysts have comparable activity and selectivity to the standard protocol when tested for the Suzuki-Miyaura cross-coupling reaction of aryl bromides or iodides with arylboronic acids.Q: